Determination of Parabens in Breast Milk Samples by Dispersive Liquid-Liquid Microextraction (DLLME) and Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry
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منابع مشابه
Determination of estrogens in water samples using dispersive liquid liquid microextraction and high performance liquid chromatography.
A new method for the analysis of estrogens including estrone (E1), 17b- estradiol (E2) and diethylstilbestrol (DES) in aqueous samples was performed using dispersive liquid liquid microextraction (DLLME) and high- performance liquid chromatography (HPLC). In order to optimize DLLME some important parameters such as type and volume of extraction and disperser solvent, extraction time, ionic stre...
متن کاملDetermination of some B Vitamins in Sour Cherry Juice Using Dispersive Liquid-liquid Microextraction Followed by High-performance Liquid Chromatography
Dispersive liquid-liquid microextraction method (DLLME) combined with high-performance liquid chromatography-ultraviolet detection (HPLC-UV) was used to determine thiamine (B1), nicotinamide (B3) and pyridoxine (B6) in sour cherry juice. This method was rapid, simple and sensitive. Separation was accomplished using a C18 column. The optimum chromatographic conditions were found to be: mobile ph...
متن کاملVortex-Assisted Inverted Dispersive Liquid-Liquid Microextraction of Naproxen from Human Plasma and Its Determination by High-Performance Liquid Chromatography
Extraction and determination of naproxen from human plasma were performed using Vortex-Assisted Inverted Dispersive Liquid-Liquid MicroExtraction (VA−IDLLME) and High-Performance Liquid Chromatography (HPLC). The parameters affecting extraction recovery such as type and volume of extraction and disperser solvents, pH of sample solution, stirring rate, extraction time and salt addition were ...
متن کاملDetermination of some B Vitamins in Sour Cherry Juice Using Dispersive Liquid-liquid Microextraction Followed by High-performance Liquid Chromatography
Dispersive liquid-liquid microextraction method (DLLME) combined with high-performance liquid chromatography-ultraviolet detection (HPLC-UV) was used to determine thiamine (B1), nicotinamide (B3) and pyridoxine (B6) in sour cherry juice. This method was rapid, simple and sensitive. Separation was accomplished using a C18 column. The optimum chromatographic conditions were found to be: mobile ph...
متن کاملPreconcentration and determination of palladium water samples by ionic liquid - dispersive liquid liquid microextraction combined with flame atomic absorption spectrometry
A simple, rapid and efficient dispersive liquid–liquid microextraction by use of ionic liquid (IL-DLLME)method, followed by flame atomic absorption spectrometry (FAAS) was developed for the preconcentrationand determination of palladium in water samples. In this method, an appropriate mixture of acetone and octylmethyl imidazolium hexafluorophosphate was injected rapidly into the aqueous sample...
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ژورنال
عنوان ژورنال: Journal of the Brazilian Chemical Society
سال: 2018
ISSN: 0103-5053,1678-4790
DOI: 10.21577/0103-5053.20180151